Information card for entry 4318325

Structure parameters

• Formula: C110 H126 Cl4 Co N9 O2
• Calculated formula: C106 H99 Co N9
• Title of publication: Synthesis, Structures, and Properties of a Series of Four-, Five-, and Six-Coordinate Cobalt(III) Triazacorrole Complexes: The First Examples of Transition Metal Corrolazines
• Authors of publication: Bobby Ramdhanie; Lev N. Zakharov; Arnold L. Rheingold; David P. Goldberg
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 4105 - 4107
• a: 16.6261 ± 0.0015 Å
• b: 18.4427 ± 0.0017 Å
• c: 19.0603 ± 0.0017 Å
• α: 87.664 ± 0.002°
• β: 68.536 ± 0.002°
• γ: 87.483 ± 0.002°
• Cell volume: 5432 ± 0.9 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1793
• Residual factor for significantly intense reflections: 0.0985
• Weighted residual factors for significantly intense reflections: 0.235
• Weighted residual factors for all reflections included in the refinement: 0.2718
• Goodness-of-fit parameter for all reflections included in the refinement: 0.867
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No