Information card for entry 4318381

Structure parameters

• Formula: C18 H29 Cl P Rh S2 Ti
• Calculated formula: C18 H29 Cl P Rh S2 Ti
• Title of publication: Sulfur-Bridged Early-Late Heterobimetallics Synthesized by Incorporation of Titanium, Vanadium, and Molybdenum into Bis(hydrosulfido) Templates of Group 9 Metals
• Authors of publication: Shigeki Kuwata; Tatsuya Nagano; Akihiro Matsubayashi; Youichi Ishii; Masanobu Hidai
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 4324 - 4330
• a: 17.275 ± 0.004 Å
• b: 8.371 ± 0.003 Å
• c: 16.143 ± 0.003 Å
• α: 90°
• β: 112.95 ± 0.01°
• γ: 90°
• Cell volume: 2149.6 ± 1 ų
• Cell temperature: 294.2 K
• Ambient diffraction temperature: 294.2 K
• Number of distinct elements: 7
• Space group number: 9
• Hermann-Mauguin space group symbol: C 1 c 1
• Hall space group symbol: C -2yc
• Residual factor for all reflections: 0.0232
• Residual factor for significantly intense reflections: 0.0232
• Weighted residual factors for significantly intense reflections: 0.0326
• Weighted residual factors for all reflections included in the refinement: 0.0326
• Goodness-of-fit parameter for all reflections included in the refinement: 2.405
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No