Information card for entry 4318808

Structure parameters

• Formula: C13 H30 Cl12 F N3
• Calculated formula: C13 H30 Cl12 F N3
• Title of publication: Hexaalkylguanidinium and 2-(Dialkylamino)-1,3-dimethylimidazolinium Trimethyldifluorosiliconates and Perfluoroalkoxides. Accidental Isolation and Molecular Structure of [C(NMe2)3]+F-.6CH2Cl2
• Authors of publication: Alexander A. Kolomeitsev; German Bissky; Jan Barten; Natalya Kalinovich; Enno Lork; Gerd-Volker Röschenthaler
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 6118 - 6124
• a: 14.2585 ± 0.0008 Å
• b: 14.2585 ± 0.0008 Å
• c: 13.0166 ± 0.0008 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 2291.8 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 148
• Hermann-Mauguin space group symbol: R -3 :H
• Hall space group symbol: -R 3
• Residual factor for all reflections: 0.0562
• Residual factor for significantly intense reflections: 0.0411
• Weighted residual factors for significantly intense reflections: 0.0954
• Weighted residual factors for all reflections included in the refinement: 0.1035
• Goodness-of-fit parameter for all reflections included in the refinement: 1.055
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No