Information card for entry 4318877

Structure parameters

• Formula: C39 H54 Cl4 Hf N2 P4 Si2
• Calculated formula: C39 H54 Cl4 Hf N2 P4 Si2
• Title of publication: Coupling of Coordinated 2-Iminophosphorano-1-phosphaallyl Leading to Bridged Iminophosphoranato Complexes of Zirconium and Hafnium
• Authors of publication: Zhong-Xia Wang; Ye-Xin Li
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 5934 - 5936
• a: 15.457 ± 0.002 Å
• b: 18.37 ± 0.003 Å
• c: 16.999 ± 0.003 Å
• α: 90°
• β: 104.379 ± 0.002°
• γ: 90°
• Cell volume: 4675.6 ± 1.3 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0375
• Residual factor for significantly intense reflections: 0.0258
• Weighted residual factors for significantly intense reflections: 0.0467
• Weighted residual factors for all reflections included in the refinement: 0.0497
• Goodness-of-fit parameter for all reflections included in the refinement: 0.94
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No