Information card for entry 4319217

Structure parameters

• Formula: C139 H142 Cl22 Mo8 N16 O32
• Calculated formula: C139 H120 Cl22.0002 Mo8 N16 O32
• Title of publication: Supramolecular Squares with Mo24+ Corners
• Authors of publication: F. Albert Cotton; Chun Lin; Carlos A. Murillo
• Journal of publication: Inorganic Chemistry
• Year of publication: 2001
• Journal volume: 40
• Pages of publication: 478 - 484
• a: 19.089 ± 0.001 Å
• b: 18.708 ± 0.001 Å
• c: 23.708 ± 0.001 Å
• α: 90°
• β: 90.7 ± 0.01°
• γ: 90°
• Cell volume: 8465.9 ± 0.7 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0999
• Residual factor for significantly intense reflections: 0.0754
• Weighted residual factors for all reflections: 0.1943
• Weighted residual factors for significantly intense reflections: 0.1723
• Goodness-of-fit parameter for all reflections: 1.09
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No