Information card for entry 4319232

Structure parameters

• Formula: C30 H64 Ga2 Ni2 Si6
• Calculated formula: C30 H64 Ga2 Ni2 Si6
• Title of publication: Reaction of Ni2Cp2(μ-CO)2 with the Alkylgallium(I) and Alkylindium(I) Compounds E4[C(SiMe3)3]4 (E = Ga, In). Insertion of E-R Groups into the Ni-Ni Bond versus Replacement of CO by the Isolobal E-R Ligands
• Authors of publication: Werner Uhl; Sandra Melle; Gernot Frenking; Michael Hartmann
• Journal of publication: Inorganic Chemistry
• Year of publication: 2001
• Journal volume: 40
• Pages of publication: 750 - 755
• a: 13.914 ± 0.003 Å
• b: 17.073 ± 0.003 Å
• c: 18.49 ± 0.004 Å
• α: 90°
• β: 106.89 ± 0.03°
• γ: 90°
• Cell volume: 4202.9 ± 1.6 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 213 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0373
• Residual factor for significantly intense reflections: 0.0263
• Weighted residual factors for significantly intense reflections: 0.0786
• Weighted residual factors for all reflections included in the refinement: 0.0883
• Goodness-of-fit parameter for all reflections included in the refinement: 0.668
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No