Information card for entry 4319616

Structure parameters

• Common name: Tris(Di(2-picolyl)(2-hydroxylato-3,5-di-tert-b
• Chemical name: Tris(Di(2-picolyl)(2-hydroxylato-3,5-di-tert-b
• Formula: C82 H106 Cl N9 O13 Zn3
• Calculated formula: C82 H102 Cl N9 O13 Zn3
• Title of publication: A Sterically Hindered N,N,O Tripod Ligand and Its Zinc Complex Chemistry
• Authors of publication: Alexander Trösch; Heinrich Vahrenkamp
• Journal of publication: Inorganic Chemistry
• Year of publication: 2001
• Journal volume: 40
• Pages of publication: 2305 - 2311
• a: 16.888 ± 0.003 Å
• b: 16.919 ± 0.003 Å
• c: 19.163 ± 0.004 Å
• α: 92.16 ± 0.03°
• β: 115.67 ± 0.03°
• γ: 106.65 ± 0.03°
• Cell volume: 4644 ± 2 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1224
• Residual factor for significantly intense reflections: 0.0699
• Weighted residual factors for significantly intense reflections: 0.2072
• Weighted residual factors for all reflections included in the refinement: 0.238
• Goodness-of-fit parameter for all reflections included in the refinement: 0.994
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No