Information card for entry 4319656

Structure parameters

• Common name: Potassium dimanganesehexacarbonylhexaniobate
• Formula: C6 H24 K6 Mn2 Nb6 O37
• Calculated formula: C6 K6 Mn2 Nb6 O37
• Title of publication: Robust, Alkali-Stable, Triscarbonyl Metal Derivatives of Hexametalate Anions, [M6O19{M'(CO)3}n](8-n)- (M = Nb, Ta; M' = Mn, Re; n= 1, 2)
• Authors of publication: Alexei V. Besserguenev; Michael H. Dickman; Michael T. Pope
• Journal of publication: Inorganic Chemistry
• Year of publication: 2001
• Journal volume: 40
• Pages of publication: 2582 - 2586
• a: 17.812 ± 0.002 Å
• b: 10.098 ± 0.0014 Å
• c: 13.1092 ± 0.0018 Å
• α: 90°
• β: 112.733 ± 0.002°
• γ: 90°
• Cell volume: 2174.7 ± 0.5 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 12
• Hermann-Mauguin space group symbol: C 1 2/m 1
• Hall space group symbol: -C 2y
• Residual factor for all reflections: 0.0553
• Residual factor for significantly intense reflections: 0.0484
• Weighted residual factors for significantly intense reflections: 0.1331
• Weighted residual factors for all reflections included in the refinement: 0.1388
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No