Information card for entry 4319658

Structure parameters

• Common name: Potassium dirheniumhexacarbonylhexaniobate
• Formula: C6 H58 K6 Nb6 O54 Re2
• Calculated formula: C6 K6 Nb6 O53.668 Re2
• Title of publication: Robust, Alkali-Stable, Triscarbonyl Metal Derivatives of Hexametalate Anions, [M6O19{M'(CO)3}n](8-n)- (M = Nb, Ta; M' = Mn, Re; n= 1, 2)
• Authors of publication: Alexei V. Besserguenev; Michael H. Dickman; Michael T. Pope
• Journal of publication: Inorganic Chemistry
• Year of publication: 2001
• Journal volume: 40
• Pages of publication: 2582 - 2586
• a: 21.8666 ± 0.0019 Å
• b: 10.3085 ± 0.0009 Å
• c: 26.78 ± 0.002 Å
• α: 90°
• β: 108.787 ± 0.001°
• γ: 90°
• Cell volume: 5714.9 ± 0.8 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0648
• Residual factor for significantly intense reflections: 0.0574
• Weighted residual factors for significantly intense reflections: 0.1622
• Weighted residual factors for all reflections included in the refinement: 0.1676
• Goodness-of-fit parameter for all reflections included in the refinement: 1.09
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No