Information card for entry 4319671

Structure parameters

• Formula: C36 H76 Li2 N4 O5 P2 S2
• Calculated formula: C36 H76 Li2 N4 O5 P2 S2
• Title of publication: Preparation and X-ray Structures of Alkali-Metal Derivatives of the Ambidentate Anions [tBuN(E)P(μ-NtBu)2P(E)NtBu]2- (E = S, Se) and [tBuN(Se)P(μ-NtBu)2PN(H)tBu)]-
• Authors of publication: Tristram Chivers; Mark Krahn; Masood Parvez; Gabriele Schatte
• Journal of publication: Inorganic Chemistry
• Year of publication: 2001
• Journal volume: 40
• Pages of publication: 2547 - 2553
• a: 13.172 ± 0.003 Å
• b: 16.877 ± 0.002 Å
• c: 10.3952 ± 0.0016 Å
• α: 91.917 ± 0.012°
• β: 90.428 ± 0.016°
• γ: 95.251 ± 0.014°
• Cell volume: 2299.8 ± 0.7 ų
• Cell temperature: 170 ± 2 K
• Ambient diffraction temperature: 170 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1281
• Residual factor for significantly intense reflections: 0.061
• Weighted residual factors for significantly intense reflections: 0.1719
• Weighted residual factors for all reflections included in the refinement: 0.2241
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No