Information card for entry 4319689

Structure parameters

• Formula: C13 H13 O S5 Sb
• Calculated formula: C13 H5 O S5 Sb
• Title of publication: Two Successive Single Crystal Phase Transitions Involving the Coordination Sphere of Antimony in PhSb(dmit), the First Organo-Antimony(III) Dithiolene Complex
• Authors of publication: Narcis Avarvari; Eric Faulques; Marc Fourmigué
• Journal of publication: Inorganic Chemistry
• Year of publication: 2001
• Journal volume: 40
• Pages of publication: 2570 - 2577
• a: 16.736 ± 0.003 Å
• b: 8.9653 ± 0.0018 Å
• c: 33.132 ± 0.007 Å
• α: 90°
• β: 91.98 ± 0.03°
• γ: 90°
• Cell volume: 4968.3 ± 1.7 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.119
• Residual factor for significantly intense reflections: 0.1029
• Weighted residual factors for significantly intense reflections: 0.2682
• Weighted residual factors for all reflections included in the refinement: 0.2813
• Goodness-of-fit parameter for all reflections included in the refinement: 1.075
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No