Information card for entry 4319974

Structure parameters

• Formula: C16 H28 Cl2 Fe N P S
• Calculated formula: C16 H28 Cl2 Fe N P S
• Title of publication: Contrasting Formation of a (Phenylthio)phosphinimine and (Phenylthio)phosphazide. Synthesis of Metal Complexes
• Authors of publication: Luc LePichon; Douglas W. Stephan
• Journal of publication: Inorganic Chemistry
• Year of publication: 2001
• Journal volume: 40
• Pages of publication: 3827 - 3829
• a: 9.3285 ± 0.0001 Å
• b: 15.2783 ± 0.0003 Å
• c: 15.072 ± 0.0002 Å
• α: 90°
• β: 102.104 ± 0.001°
• γ: 90°
• Cell volume: 2100.36 ± 0.06 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0517
• Residual factor for significantly intense reflections: 0.0478
• Weighted residual factors for significantly intense reflections: 0.1202
• Weighted residual factors for all reflections included in the refinement: 0.1225
• Goodness-of-fit parameter for all reflections included in the refinement: 1.167
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No