Information card for entry 4320006

Structure parameters

• Formula: C33 H25 Cl N5 O5 Os
• Calculated formula: C33 H25 Cl N5 O5 Os
• SMILES: [Os]123([n]4ccccc4c4[n]1cccc4)([n]1ccccc1c1[n]2cccc1)N(C(=O)c1ccccc31)c1ccccc1.Cl(=O)(=O)(=O)[O-]
• Title of publication: Unusual Transformation of N-Arylbenzohydroxamic Acids Mediated by Osmium. Formation of Organometallic Complexes of Osmium(III)
• Authors of publication: Anindya Das; Falguni Basuli; Larry R. Falvello; Samaresh Bhattacharya
• Journal of publication: Inorganic Chemistry
• Year of publication: 2001
• Journal volume: 40
• Pages of publication: 4085 - 4088
• a: 10.66 ± 0.005 Å
• b: 14.99 ± 0.004 Å
• c: 18.662 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2982.1 ± 1.7 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 297 ± 2 K
• Number of distinct elements: 6
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0922
• Residual factor for significantly intense reflections: 0.0558
• Weighted residual factors for significantly intense reflections: 0.1253
• Weighted residual factors for all reflections included in the refinement: 0.1426
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No