Information card for entry 4320032

Structure parameters

• Formula: C24 H43 Cl N5 Si2 Ta
• Calculated formula: C24 H43 Cl N5 Si2 Ta
• SMILES: [Ta]12(=NC(C)(C)C)(N([Si](C)(C)C)CC(c3[n]2cccc3)(CN1[Si](C)(C)C)C)([n]1ccccc1)Cl
• Title of publication: Group 5 Imido Complexes Derived from Diamido-Pyridine Ligands
• Authors of publication: Stephen M. Pugh; Alexander J. Blake; Lutz H. Gade; Philip Mountford
• Journal of publication: Inorganic Chemistry
• Year of publication: 2001
• Journal volume: 40
• Pages of publication: 3992 - 4001
• a: 15.56 ± 0.005 Å
• b: 16.571 ± 0.004 Å
• c: 22.319 ± 0.006 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5755 ± 3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0734
• Residual factor for significantly intense reflections: 0.0526
• Weighted residual factors for significantly intense reflections: 0.1215
• Weighted residual factors for all reflections included in the refinement: 0.1446
• Goodness-of-fit parameter for all reflections included in the refinement: 1.19
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No