Crystallography Open Database

Information card for entry 4320190

4320189 << 4320190 >> 4320191

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Structure parameters

Formula	C63 H74 Cl6 Li2 O8 Sm2
Calculated formula	C63 H74 Cl6 Li2 O8 Sm2
Title of publication	Synthesis and X-ray Crystal Structure Determination of First Examples of Donor-Functionalized Terphenyl Lanthanide Complexes
Authors of publication	Gerd W. Rabe; Christian D. Bérubé; Glenn P. A. Yap
Journal of publication	Inorganic Chemistry
Year of publication	2001
Journal volume	40
Pages of publication	4780 - 4784
a	10.3457 ± 0.0008 Å
b	12.5658 ± 0.001 Å
c	14.4365 ± 0.0011 Å
α	70.225 ± 0.001°
β	81.282 ± 0.001°
γ	66.833 ± 0.001°
Cell volume	1623.3 ± 0.2 Å³
Cell temperature	203 ± 2 K
Ambient diffraction temperature	203 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.043
Residual factor for significantly intense reflections	0.034
Weighted residual factors for significantly intense reflections	0.0705
Weighted residual factors for all reflections included in the refinement	0.0712
Goodness-of-fit parameter for all reflections included in the refinement	1.033
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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