Information card for entry 4320194

Structure parameters

• Formula: C124 H244 Cl6 N40 Ni9 O22.5
• Calculated formula: C124 H244 Cl6 N40 Ni9 O22.5
• Title of publication: Extremely Bent Cyanide Coordination at a Preorganized Dinickel Site and Assembly of a Starlike Nonanuclear Complex from the Constrained Dinickel Building Blocks
• Authors of publication: Franc Meyer; Rainer F. Winter; Elisabeth Kaifer
• Journal of publication: Inorganic Chemistry
• Year of publication: 2001
• Journal volume: 40
• Pages of publication: 4597 - 4603
• a: 20.593 ± 0.004 Å
• b: 20.793 ± 0.004 Å
• c: 21.034 ± 0.004 Å
• α: 90.79 ± 0.03°
• β: 95.78 ± 0.03°
• γ: 110.32 ± 0.03°
• Cell volume: 8392 ± 3 ų
• Cell temperature: 200 K
• Ambient diffraction temperature: 200 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1963
• Residual factor for significantly intense reflections: 0.0829
• Weighted residual factors for significantly intense reflections: 0.22
• Weighted residual factors for all reflections included in the refinement: 0.2692
• Goodness-of-fit parameter for all reflections included in the refinement: 1
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No