Information card for entry 4320235

Structure parameters

• Formula: C18 H17 Cl1.86 O7.14 W
• Calculated formula: C18 H17 Cl1.93 O7 W
• Title of publication: Tungsten Oxo Salicylate Complexes from Tungsten Hexachloride Reactions Systems
• Authors of publication: Vladimir Kolesnichenko; Mark H. Mason; Jeff B. Botts; Alix M. Botts; Timothy E. Baroni; Joseph A. Heppert; Arnold L. Rheingold; Louise Liable-Sands; Glenn P. A. Yap
• Journal of publication: Inorganic Chemistry
• Year of publication: 2001
• Journal volume: 40
• Pages of publication: 5010 - 5016
• a: 9.9701 ± 0.0001 Å
• b: 15.6703 ± 0.0001 Å
• c: 12.5001 ± 0.0002 Å
• α: 90°
• β: 93.566 ± 0.001°
• γ: 90°
• Cell volume: 1949.17 ± 0.04 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0299
• Residual factor for significantly intense reflections: 0.0232
• Weighted residual factors for significantly intense reflections: 0.0573
• Weighted residual factors for all reflections included in the refinement: 0.0594
• Goodness-of-fit parameter for all reflections included in the refinement: 1.01
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No