Information card for entry 4320249

Structure parameters

• Formula: C60 H116 Fe2 N24 Ni3 O13
• Calculated formula: C60 Fe2 N24 Ni3 O13
• Title of publication: Cyano-Bridged Bimetallic Assemblies from Hexacyanometalate, [M(CN)6]3- (M = MnIII and FeIII), and [M(N4-macrocycle)]2+ (M = FeIII, NiII and ZnII) Building Blocks. Syntheses, Multidimensional Structures, and Magnetic Properties
• Authors of publication: Enrique Colacio; Mustapha Ghazi; Helen Stoeckli-Evans; Francesc Lloret; José María Moreno; Cristina Pérez
• Journal of publication: Inorganic Chemistry
• Year of publication: 2001
• Journal volume: 40
• Pages of publication: 4876 - 4883
• a: 20.462 ± 0.007 Å
• b: 16.292 ± 0.004 Å
• c: 27.262 ± 0.007 Å
• α: 90°
• β: 101.29 ± 0.04°
• γ: 90°
• Cell volume: 8912 ± 5 ų
• Cell temperature: 203 ± 2 K
• Ambient diffraction temperature: 203 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: A 1 2/n 1
• Hall space group symbol: -A 2yab
• Residual factor for all reflections: 0.4071
• Residual factor for significantly intense reflections: 0.139
• Weighted residual factors for significantly intense reflections: 0.2337
• Weighted residual factors for all reflections included in the refinement: 0.3751
• Goodness-of-fit parameter for all reflections included in the refinement: 0.546
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No