Information card for entry 4320279

Structure parameters

• Formula: C26 H44 B Cl2 F4 O P4 Rh
• Calculated formula: C26 H44 B Cl2 F4 O P4 Rh
• Title of publication: A Monometallic Rh(III) Tetraphosphine Complex: Reductive Activation of CH2Cl2 and Selective Meso to Racemic Tetraphosphine Ligand Isomerization
• Authors of publication: Clinton Hunt; Frank R. Fronczek; Damon R. Billodeaux; George G. Stanley
• Journal of publication: Inorganic Chemistry
• Year of publication: 2001
• Journal volume: 40
• Pages of publication: 5192 - 5198
• a: 10.712 ± 0.001 Å
• b: 14.467 ± 0.002 Å
• c: 21.619 ± 0.001 Å
• α: 90°
• β: 98.21 ± 0.01°
• γ: 90°
• Cell volume: 3316 ± 0.6 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.037
• Residual factor for significantly intense reflections: 0.03
• Weighted residual factors for all reflections: 0.046
• Weighted residual factors for significantly intense reflections: 0.038
• Goodness-of-fit parameter for all reflections: 1.281
• Goodness-of-fit parameter for significantly intense reflections: 1.084
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: Mo-Kα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No