Information card for entry 4320632

Structure parameters

• Chemical name: Tetraphenylarsonium trans-bis(heptacyanomolybdenum(IV) -u-oxo-)bis(ethylenediammine)Osmate(VI)
• Formula: C118 H108 As4 Mo2 N18 O11 Os
• Calculated formula: C118 H106.5 As4 Mo2 N18 O10.5 Os
• Title of publication: Reaction of [Os(en)2O2]2+ with Photolyzed [Mo(CN)8]4- in Water
• Authors of publication: R. Kent Murmann; Charles L. Barnes
• Journal of publication: Inorganic Chemistry
• Year of publication: 2001
• Journal volume: 40
• Pages of publication: 6514 - 6517
• a: 10.978 ± 0.005 Å
• b: 13.17 ± 0.005 Å
• c: 40.322 ± 0.017 Å
• α: 93.501 ± 0.007°
• β: 95.994 ± 0.007°
• γ: 95.638 ± 0.008°
• Cell volume: 5755 ± 4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0759
• Residual factor for significantly intense reflections: 0.0639
• Weighted residual factors for significantly intense reflections: 0.1214
• Weighted residual factors for all reflections included in the refinement: 0.1265
• Goodness-of-fit parameter for all reflections included in the refinement: 1.262
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No