Information card for entry 4320805

Structure parameters

• Formula: C12 H30 Cl4 Os2 P2 Re4 Se8
• Calculated formula: C12 H30 Cl4 Os2 P2 Re4 Se8
• SMILES: C(C)[P](CC)(CC)[Os]1234567[Re]89%10%11%12%13(Cl)[Se]1[Re]1%14%15%1629(Cl)[Os]29%17%188([P](CC)(CC)CC)([Re]8%193%10(Cl)([Re]412(Cl)([Se]58)([Se]%159)([Se]%17%19)[Se]7%16)([Se]6%12)[Se]%13%18)[Se]%11%14
• Title of publication: Heterometal Substitution in the Dimensional Reduction of Cluster Frameworks: Synthesis of Soluble [Re6-nOsnSe8Cl6](4-n) (n = 1-3) Cluster-Containing Solids
• Authors of publication: Eric G. Tulsky; Jeffrey R. Long
• Journal of publication: Inorganic Chemistry
• Year of publication: 2001
• Journal volume: 40
• Pages of publication: 6990 - 7002
• a: 9.2771 ± 0.0003 Å
• b: 11.7511 ± 0.0004 Å
• c: 15.197 ± 0.0005 Å
• α: 90°
• β: 103.884 ± 0.002°
• γ: 90°
• Cell volume: 1608.31 ± 0.09 ų
• Cell temperature: 152 ± 2 K
• Ambient diffraction temperature: 152 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0572
• Residual factor for significantly intense reflections: 0.0377
• Weighted residual factors for all reflections: 0.0917
• Weighted residual factors for significantly intense reflections: 0.0861
• Goodness-of-fit parameter for all reflections: 0.98
• Goodness-of-fit parameter for significantly intense reflections: 1.088
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No