Information card for entry 4320812

Structure parameters

• Formula: C10.73 H17.46 K6 O23 S4 W3
• Calculated formula: C9.36 H9 K5 O20.5 S3 W2.5
• Title of publication: Preparation and Crystal Structures of Formato Complexes of the [M^IV^~3~O~4~]^4+^ and [M^IV^~3~S~4~]^4+^ (M = Mo,W) Clusters. Convenient Precursors to the Corresponding Aqua Complexes
• Authors of publication: Michael Brorson; Alan Hazell; Claus J. H. Jacobsen; Iver Schmidt; Jørgen Villadsen
• Journal of publication: Inorganic Chemistry
• Year of publication: 2000
• Journal volume: 39
• Pages of publication: 1346 - 1350
• a: 19.605 ± 0.006 Å
• b: 14.458 ± 0.007 Å
• c: 13.627 ± 0.005 Å
• α: 90°
• β: 118.94 ± 0.02°
• γ: 90°
• Cell volume: 3380 ± 2 ų
• Cell temperature: 294 K
• Ambient diffraction temperature: 294 K
• Number of distinct elements: 6
• Space group number: 12
• Hermann-Mauguin space group symbol: C 1 2/m 1
• Hall space group symbol: -C 2y
• Residual factor for significantly intense reflections: 0.046
• Weighted residual factors for significantly intense reflections: 0.055
• Goodness-of-fit parameter for significantly intense reflections: 1.224
• Diffraction radiation wavelength: 0.56087 Å
• Diffraction radiation type: AgKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No