Information card for entry 4320818

Structure parameters

• Formula: C66 H132 N21 Nd3 O39
• Calculated formula: C66 H97 N21 Nd3 O39
• Title of publication: Crystallographic, X-ray Absorption, and IR Studies of Solid- and Solution-State Structures of Tris(nitrato)N,N,N',N'-Tetraethylmalonamide Complexes of Lanthanides. Comparison with the Americium Complex
• Authors of publication: C. Den Auwer; M. C. Charbonnel; M. G. B. Drew; M. Grigoriev; M. J. Hudson; P. B. Iveson; C. Madic; M. Nierlich; M. T. Presson; R. Revel; M. L. Russell; P. Thuéry
• Journal of publication: Inorganic Chemistry
• Year of publication: 2000
• Journal volume: 39
• Pages of publication: 1487 - 1495
• a: 11.2627 ± 0.0004 Å
• b: 20.5992 ± 0.0008 Å
• c: 22.2126 ± 0.0008 Å
• α: 90°
• β: 102.572 ± 0.001°
• γ: 90°
• Cell volume: 5029.8 ± 0.3 ų
• Cell temperature: 273 ± 2 K
• Ambient diffraction temperature: 273 ± 2 K
• Number of distinct elements: 5
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0608
• Residual factor for significantly intense reflections: 0.0351
• Weighted residual factors for all reflections: 0.1115
• Weighted residual factors for all reflections included in the refinement: 0.0822
• Goodness-of-fit parameter for all reflections: 1.008
• Goodness-of-fit parameter for all reflections included in the refinement: 1.055
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No