Information card for entry 4320820

Structure parameters

• Formula: C19 H21 Mo N6 O3 Si
• Calculated formula: C19 H21 Mo N6 O3 Si
• Title of publication: Syntheses and Structures of Methyltris(pyrazolyl)silane Complexes of the Group 6 Metals
• Authors of publication: Eric E. Pullen; Daniel Rabinovich; Christopher D. Incarvito; Thomas E. Concolino; Arnold L. Rheingold
• Journal of publication: Inorganic Chemistry
• Year of publication: 2000
• Journal volume: 39
• Pages of publication: 1561 - 1567
• a: 18.6624 ± 0.0004 Å
• b: 14.1761 ± 0.0002 Å
• c: 8.4402 ± 0.0002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2232.94 ± 0.08 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.0412
• Residual factor for significantly intense reflections: 0.0359
• Weighted residual factors for significantly intense reflections: 0.1269
• Weighted residual factors for all reflections included in the refinement: 0.1337
• Goodness-of-fit parameter for all reflections included in the refinement: 1.17
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No