Information card for entry 4320852

Structure parameters

• Common name: [Cs(NO3).Ni(3-MeOsal1,3pn)]3.MeOH
• Chemical name: [Caesium nitrate / N.N'-bis(3-methoxysalicylidene) propane-1,3-diaminatonickel(II)] (1/1)] /methanol (1/1).
• Formula: C58 H56 Cs3 N9 Ni3 O22
• Calculated formula: C58 H56 Cs3 N9 Ni3 O22
• Title of publication: Adduct Formation between Alkali Metal Ions and Divalent Metal Salicylaldimine Complexes Having Methoxy Substituents. A Structural Investigation
• Authors of publication: D. Cunningham; P. McArdle; M. Mitchell; N. Ní Chonchubhair; M. O'Gara; Federico Franceschi; Carlo Floriani
• Journal of publication: Inorganic Chemistry
• Year of publication: 2000
• Journal volume: 39
• Pages of publication: 1639 - 1649
• a: 12.591 ± 0.0002 Å
• b: 23.488 ± 0.0002 Å
• c: 22.666 ± 0.0002 Å
• α: 90 ± 0.0001°
• β: 99.35 ± 0.0001°
• γ: 90 ± 0.0001°
• Cell volume: 6614.13 ± 0.13 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1118
• Residual factor for significantly intense reflections: 0.0657
• Weighted residual factors for significantly intense reflections: 0.1875
• Weighted residual factors for all reflections included in the refinement: 0.21
• Goodness-of-fit parameter for all reflections included in the refinement: 0.976
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No