Information card for entry 4320990

Structure parameters

• Common name: Phenyl[tris(2-thio-3-trimethylsilylphenyl-k3S)phosphine-kP]tin
• Chemical name: Phenyl[tris(2-thio-3-trimethylsilylphenyl-k3S)phosphine-kP]tin
• Formula: C33 H41 P S3 Si3 Sn
• Calculated formula: C33 H41 P S3 Si3 Sn
• SMILES: [Sn]123([P](c4c(S1)c(ccc4)[Si](C)(C)C)(c1c(S2)c(ccc1)[Si](C)(C)C)c1c(S3)c(ccc1)[Si](C)(C)C)c1ccccc1
• Title of publication: Synthesis, Characterization, Crystal Structures, and Reactions of Trigonal Bipyramidal Tin(IV) Complexes Containing a Tetradentate Tripodal Tristhiolatophosphine Ligand. Use in the One-Step Synthesis of an Iron(IV) Complex
• Authors of publication: Kerry A. (Fusie) Clark; T. Adrian George; Tom J. Brett; Charles R. Ross; Richard K. Shoemaker
• Journal of publication: Inorganic Chemistry
• Year of publication: 2000
• Journal volume: 39
• Pages of publication: 2252 - 2253
• a: 10.111 ± 0.002 Å
• b: 14.737 ± 0.003 Å
• c: 15.342 ± 0.003 Å
• α: 112.86 ± 0.03°
• β: 107.21 ± 0.03°
• γ: 90.75 ± 0.03°
• Cell volume: 1990.8 ± 1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0681
• Residual factor for significantly intense reflections: 0.0556
• Weighted residual factors for significantly intense reflections: 0.1418
• Weighted residual factors for all reflections included in the refinement: 0.1533
• Goodness-of-fit parameter for all reflections included in the refinement: 1.127
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No