Information card for entry 4321013

Structure parameters

• Formula: C55 H43 O5 P3 Pd S2 W
• Calculated formula: C55 H43 O5 P3 Pd S2 W
• Title of publication: Synthesis and Structural Characterization of Configurational Isomers of Tungsten-Palladium Complexes with Bridging Diphenyl(dithioalkoxycarbonyl)phosphine as a Ligand and Phosphine Transfer from Tungsten to Palladium
• Authors of publication: Kuang-Hway Yih; Gene-Hsiang Lee; Yu Wang
• Journal of publication: Inorganic Chemistry
• Year of publication: 2000
• Journal volume: 39
• Pages of publication: 2445 - 2451
• a: 10.92 ± 0.003 Å
• b: 14.707 ± 0.005 Å
• c: 16.654 ± 0.005 Å
• α: 99.98 ± 0.03°
• β: 93.75 ± 0.03°
• γ: 99.44 ± 0.03°
• Cell volume: 2586.3 ± 1.4 ų
• Cell temperature: 298 K
• Ambient diffraction temperature: 298 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.069
• Residual factor for significantly intense reflections: 0.04
• Weighted residual factors for all reflections: 0.044
• Weighted residual factors for significantly intense reflections: 0.042
• Goodness-of-fit parameter for significantly intense reflections: 1.68
• Diffraction radiation wavelength: 0.7093 Å
• Diffraction radiation type: MolybdenumKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No