Information card for entry 4321028

Structure parameters

• Formula: C16 H37 Li3 N4 O Si
• Calculated formula: C16 H37 Li3 N4 O Si
• Title of publication: Polylithiated Tetraaminosilanes: Synthesis and Characterization of (Et2O.Li)4[Si(Nnaph)4] and X-ray Structure of {THF.Li3[Si(NiPr)3(NHiPr)]}2
• Authors of publication: Justin K. Brask; Tristram Chivers; Masood Parvez
• Journal of publication: Inorganic Chemistry
• Year of publication: 2000
• Journal volume: 39
• Pages of publication: 2505 - 2508
• a: 10.661 ± 0.007 Å
• b: 16.964 ± 0.005 Å
• c: 12.405 ± 0.004 Å
• α: 90°
• β: 93.22 ± 0.04°
• γ: 90°
• Cell volume: 2239.9 ± 1.8 ų
• Cell temperature: 170 ± 1 K
• Ambient diffraction temperature: 170 ± 1 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0614
• Residual factor for significantly intense reflections: 0.0614
• Weighted residual factors for all reflections: 0.0611
• Weighted residual factors for significantly intense reflections: 0.0611
• Goodness-of-fit parameter for all reflections: 2.319
• Goodness-of-fit parameter for significantly intense reflections: 2.319
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No