Information card for entry 4321059

Structure parameters

• Chemical name: [WOS(OSiPh3)2(Me4phen)
• Formula: C52 H46 N2 O3 S Si2 W
• Calculated formula: C52 H46 N2 O3 S Si2 W
• Title of publication: Oxo/Sulfidotungstate(VI) as Precursors to WVIO2, WVIOS, and WVIS2 Complexes and WIV-Dithiolene Chelate Rings
• Authors of publication: Mingming Miao; Michael W. Willer; R. H. Holm
• Journal of publication: Inorganic Chemistry
• Year of publication: 2000
• Journal volume: 39
• Pages of publication: 2843 - 2849
• a: 16.7097 ± 0.0015 Å
• b: 10.3575 ± 0.0006 Å
• c: 27.002 ± 0.003 Å
• α: 90°
• β: 103.518 ± 0.009°
• γ: 90°
• Cell volume: 4543.8 ± 0.7 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0334
• Residual factor for significantly intense reflections: 0.0305
• Weighted residual factors for significantly intense reflections: 0.076
• Weighted residual factors for all reflections included in the refinement: 0.0772
• Goodness-of-fit parameter for all reflections included in the refinement: 1.08
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No