Information card for entry 4321081

Structure parameters

• Formula: As2 Cl4 F30 O6 Te6
• Calculated formula: As2 Cl4 F30 O6 Te6
• Title of publication: Tetrachloro- and Tetrabromoarsonium(V) Cations: Raman and 75As, 19F NMR Spectroscopic Characterization and X-ray Crystal Structures of [AsCl4][As(OTeF5)6] and [AsBr4][AsF(OTeF5)5]
• Authors of publication: Michael Gerken; Peter Kolb; Andreas Wegner; Hélène P. A. Mercier; Horst Borrmann; David A. Dixon; Gary J. Schrobilgen
• Journal of publication: Inorganic Chemistry
• Year of publication: 2000
• Journal volume: 39
• Pages of publication: 2813 - 2824
• a: 9.8741 ± 0.0014 Å
• b: 9.8741 ± 0.0014 Å
• c: 55.301 ± 0.011 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 4669.4 ± 1.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 148
• Hermann-Mauguin space group symbol: R -3 :H
• Hall space group symbol: -R 3
• Residual factor for all reflections: 0.0443
• Residual factor for significantly intense reflections: 0.0438
• Weighted residual factors for all reflections: 0.1447
• Weighted residual factors for significantly intense reflections: 0.1444
• Goodness-of-fit parameter for all reflections: 2.184
• Goodness-of-fit parameter for significantly intense reflections: 2.189
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No