Information card for entry 4321298

Structure parameters

• Formula: C34 H60 F9 N5 O23 P4 Ru2 S5
• Calculated formula: C34 H42 F9 N5 O23 P4 Ru2 S5
• Title of publication: Syntheses of Ketonated Disulfide-Bridged Diruthenium Complexes via C-H Bond Activation and C-S Bond Formation
• Authors of publication: Hiroyasu Sugiyama; Md. Munkir Hossain; Yong-Shou Lin; Kazuko Matsumoto
• Journal of publication: Inorganic Chemistry
• Year of publication: 2000
• Journal volume: 39
• Pages of publication: 3948 - 3956
• a: 15.7178 ± 0.0007 Å
• b: 24.4198 ± 0.0011 Å
• c: 16.8492 ± 0.0008 Å
• α: 90°
• β: 90.831 ± 0.001°
• γ: 90°
• Cell volume: 6466.5 ± 0.5 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0961
• Residual factor for significantly intense reflections: 0.0659
• Weighted residual factors for significantly intense reflections: 0.1953
• Weighted residual factors for all reflections included in the refinement: 0.2191
• Goodness-of-fit parameter for all reflections included in the refinement: 1.011
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No