Information card for entry 4321459

Structure parameters

• Formula: C30 H28 Cl3 N4 O2.5 P Re
• Calculated formula: C30 H28 Cl3 N4 O2.5 P Re
• Title of publication: Preparation and Characterization of Oxorhenium(V) Complexes with 2,2'-Biimidazole: The Strong Affinity of Coordinated Biimidazole for Chloride Ions via N-H...Cl-Hydrogen Bonding
• Authors of publication: Sébastien Fortin; André L. Beauchamp
• Journal of publication: Inorganic Chemistry
• Year of publication: 2000
• Journal volume: 39
• Pages of publication: 4886 - 4893
• a: 10.323 ± 0.003 Å
• b: 11.794 ± 0.003 Å
• c: 13.548 ± 0.004 Å
• α: 86.22 ± 0.02°
• β: 83.63 ± 0.02°
• γ: 71.64 ± 0.02°
• Cell volume: 1555 ± 0.8 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0585
• Residual factor for significantly intense reflections: 0.0554
• Weighted residual factors for all reflections: 0.1573
• Weighted residual factors for all reflections included in the refinement: 0.1547
• Goodness-of-fit parameter for all reflections: 1.044
• Goodness-of-fit parameter for all reflections included in the refinement: 1.08
• Diffraction radiation wavelength: 1.54056 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No