Structural Diversity in Solvated Lithium Aryloxides. Syntheses, Characterization, and Structures of [Li(OAr)(THF)x]n and [Li(OAr)(py)x]2 Complexes Where OAr = OC6H5, OC6H4(2-Me), OC6H3(2,6-(Me))2, OC6H4(2-Pri), OC6H3(2,6-(Pri))2, OC6H4(2-But), OC6H3(2,6-(But))2
Authors of publication
Timothy J. Boyle; Dawn M. Pedrotty; Todd M. Alam; Sara C. Vick; Mark A. Rodriguez
Journal of publication
Inorganic Chemistry
Year of publication
2000
Journal volume
39
Pages of publication
5133 - 5146
a
26.89 ± 0.003 Å
b
9.2373 ± 0.0009 Å
c
19.761 ± 0.002 Å
α
90°
β
124.812 ± 0.005°
γ
90°
Cell volume
4030 ± 0.8 Å3
Cell temperature
168 ± 2 K
Ambient diffraction temperature
168 ± 2 K
Number of distinct elements
4
Space group number
15
Hermann-Mauguin space group symbol
C 1 2/c 1
Hall space group symbol
-C 2yc
Residual factor for all reflections
0.157
Residual factor for significantly intense reflections
0.0541
Weighted residual factors for significantly intense reflections
0.1252
Weighted residual factors for all reflections included in the refinement
0.1582
Goodness-of-fit parameter for all reflections included in the refinement
