Structural Diversity in Solvated Lithium Aryloxides. Syntheses, Characterization, and Structures of [Li(OAr)(THF)x]n and [Li(OAr)(py)x]2 Complexes Where OAr = OC6H5, OC6H4(2-Me), OC6H3(2,6-(Me))2, OC6H4(2-Pri), OC6H3(2,6-(Pri))2, OC6H4(2-But), OC6H3(2,6-(But))2
Authors of publication
Timothy J. Boyle; Dawn M. Pedrotty; Todd M. Alam; Sara C. Vick; Mark A. Rodriguez
Journal of publication
Inorganic Chemistry
Year of publication
2000
Journal volume
39
Pages of publication
5133 - 5146
a
9.151 ± 0.0007 Å
b
14.4287 ± 0.0012 Å
c
14.1346 ± 0.0012 Å
α
90°
β
105.326 ± 0.001°
γ
90°
Cell volume
1799.9 ± 0.3 Å3
Cell temperature
293 ± 2 K
Ambient diffraction temperature
293 ± 2 K
Number of distinct elements
4
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/n 1
Hall space group symbol
-P 2yn
Residual factor for all reflections
0.0916
Residual factor for significantly intense reflections
0.0527
Weighted residual factors for significantly intense reflections
0.1471
Weighted residual factors for all reflections included in the refinement
0.1724
Goodness-of-fit parameter for all reflections included in the refinement
