Information card for entry 4321655

Structure parameters

• Formula: C19 H27 B Cl N10 O2 Re Si
• Calculated formula: C19 H27 B Cl N10 O2 Re Si
• Title of publication: Cationic Re(V) Oxo Complexes with Poly(pyrazolyl)borates: Synthesis, Characterization, and Stability
• Authors of publication: António Paulo; Ângela Domingos; Raquel Garcia; Isabel Santos
• Journal of publication: Inorganic Chemistry
• Year of publication: 2000
• Journal volume: 39
• Pages of publication: 5669 - 5674
• a: 16.356 ± 0.002 Å
• b: 20.384 ± 0.003 Å
• c: 17.36 ± 0.003 Å
• α: 90°
• β: 106.971 ± 0.012°
• γ: 90°
• Cell volume: 5535.8 ± 1.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.2158
• Residual factor for significantly intense reflections: 0.0852
• Weighted residual factors for all reflections: 0.1594
• Weighted residual factors for significantly intense reflections: 0.0972
• Goodness-of-fit parameter for all reflections: 1.079
• Goodness-of-fit parameter for significantly intense reflections: 1.201
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No