Information card for entry 4321657

Structure parameters

• Formula: C17 H27 Cl2 Cu N5 O8
• Calculated formula: C17 H27 Cl2 Cu N5 O8
• Title of publication: Synthesis and Crystal Structure Determination of Some Asymmetrical and Symmetrical CR-Type Macrocyclic Schiff Base Complexes, with a Single Pendant Coordinating 2-Aminoethyl Arm
• Authors of publication: Hassan Keypour; Sadegh Salehzadeh; Robin G. Pritchard; R. V. Parish
• Journal of publication: Inorganic Chemistry
• Year of publication: 2000
• Journal volume: 39
• Pages of publication: 5787 - 5790
• a: 7.8764 ± 0.001 Å
• b: 15.361 ± 0.002 Å
• c: 19.37 ± 0.002 Å
• α: 90°
• β: 100.33 ± 0.01°
• γ: 90°
• Cell volume: 2305.6 ± 0.5 ų
• Cell temperature: 295 ± 2 K
• Ambient diffraction temperature: 295 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1474
• Residual factor for significantly intense reflections: 0.0537
• Weighted residual factors for significantly intense reflections: 0.1397
• Weighted residual factors for all reflections included in the refinement: 0.1859
• Goodness-of-fit parameter for all reflections included in the refinement: 0.996
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No