Information card for entry 4321698

Structure parameters

• Formula: C23 H25 B N8 O Re
• Calculated formula: C23 H25 B N8 O Re
• Title of publication: {TpRe(bpy)}: A Novel Pentaaminerhenium System That Stabilizes Both High and Low Oxidation States (Tp = Hydridotris(pyrazolyl)borate; bpy = 2,2'-Bipyridyl)
• Authors of publication: T. Brent Gunnoe; Scott H. Meiere; Michal Sabat; W. Dean Harman
• Journal of publication: Inorganic Chemistry
• Year of publication: 2000
• Journal volume: 39
• Pages of publication: 6127 - 6130
• a: 10.1935 ± 0.0005 Å
• b: 18.307 ± 0.0009 Å
• c: 12.5987 ± 0.0006 Å
• α: 90°
• β: 96.299 ± 0.001°
• γ: 90°
• Cell volume: 2336.9 ± 0.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0347
• Residual factor for significantly intense reflections: 0.03
• Weighted residual factors for significantly intense reflections: 0.0602
• Weighted residual factors for all reflections included in the refinement: 0.061
• Goodness-of-fit parameter for all reflections included in the refinement: 1.042
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No