Information card for entry 4322035

Structure parameters

• Chemical name: Mer-trichloro-tris(propylamine)-molybdenum(III)
• Formula: C9.67 H28.33 Cl3 Mo N3 O0.17
• Calculated formula: C9.66667 H28.3333 Cl3 Mo N3 O0.166667
• Title of publication: Mixed Chloride/Amine Complexes of Dimolybdenum(II,II). 3. Preparation, Characterization, and Crystal Structure of Mo2Cl4(NH2R)4 (R = Et, Prn, But, Cy): First Quadruply-Bonded Dimolybdenum Compounds with Primary Amine Ligands
• Authors of publication: F. Albert Cotton; Evgeny V. Dikarev; Santiago Herrero
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 2649 - 2654
• a: 12.37 ± 0.002 Å
• b: 17.977 ± 0.002 Å
• c: 25.498 ± 0.006 Å
• α: 95.32 ± 0.01°
• β: 103.21 ± 0.02°
• γ: 103.48 ± 0.01°
• Cell volume: 5303.8 ± 1.7 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0869
• Residual factor for significantly intense reflections: 0.0551
• Weighted residual factors for all reflections: 0.1579
• Weighted residual factors for significantly intense reflections: 0.1386
• Goodness-of-fit parameter for all reflections: 1.033
• Goodness-of-fit parameter for significantly intense reflections: 1.076
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No