Information card for entry 4322054

Structure parameters

• Formula: C91.5 H135 Cl3 Fe2 N6 O16.5 S6 Sn
• Calculated formula: C91.5 H126 Cl3 Fe2 N6 O16.5 S6 Sn
• Title of publication: Sn(III) and Ge(III) in the Thiophenolato-Bridged Complexes [LFeSnFeL]n+ and [LFeGeFeL]n+ (n = 2, 3; L = 1,4,7-(4-tert-Butyl-2-mercaptobenzyl)-1,4,7-triazacyclononane)
• Authors of publication: Thorsten Glaser; Eckhard Bill; Thomas Weyhermüller; Wolfram Meyer-Klaucke; Karl Wieghardt
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 2632 - 2642
• a: 15.772 ± 0.002 Å
• b: 17.527 ± 0.002 Å
• c: 20.096 ± 0.003 Å
• α: 72.95 ± 0.02°
• β: 79.09 ± 0.02°
• γ: 68.5 ± 0.02°
• Cell volume: 4920.6 ± 1.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0957
• Residual factor for significantly intense reflections: 0.0558
• Weighted residual factors for all reflections: 0.1536
• Weighted residual factors for significantly intense reflections: 0.1098
• Goodness-of-fit parameter for all reflections: 1.103
• Goodness-of-fit parameter for significantly intense reflections: 1.012
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No