Crystallography Open Database

Information card for entry 4322329

Preview

Coordinates	4322329.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C82 H170 Cl4 F24 N4 P10 Re12 Sb4 Se16
Calculated formula	C81 H167.5 Cl4 F24 N4 P10 Re12 Sb4 Se16
Title of publication	Synthesis and Structures of Solvated Monoclusters and Bridged Di- and Triclusters Based on the cubic Building Block [Re6(μ3-Se)8]2+
Authors of publication	Zhiping Zheng; Thomas G. Gray; R. H. Holm
Journal of publication	Inorganic Chemistry
Year of publication	1999
Journal volume	38
Pages of publication	4888 - 4895
a	16.982 ± 0.0003 Å
b	18.9644 ± 0.0004 Å
c	23.2488 ± 0.0001 Å
α	97.449 ± 0.001°
β	96.387 ± 0.001°
γ	96.211 ± 0.001°
Cell volume	7320.7 ± 0.2 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	9
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1039
Residual factor for significantly intense reflections	0.0649
Weighted residual factors for all reflections	0.1563
Weighted residual factors for significantly intense reflections	0.1255
Goodness-of-fit parameter for all reflections	1.121
Goodness-of-fit parameter for significantly intense reflections	1.127
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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