Information card for entry 4322592

Structure parameters

• Formula: C22 H40 F6 N4 O6 S2 Zn
• Calculated formula: C20 H40 N4 Zn
• Title of publication: A Homologous Series of Homoleptic Zinc Bis(1,4-di-tert-butyl-1,4-diaza-1,3-butadiene) Complexes: Kx[Zn(t-BuNCHCHN-t-Bu)2], Zn(t-BuNCHCHN-t-Bu)2, and [Zn(t-BuNCHCHN-t-Bu)2](OTf)x (x = 1, 2)
• Authors of publication: Evelien Rijnberg; Bodo Richter; Karl-H. Thiele; Jaap Boersma; Nora Veldman; Anthony L. Spek; Gerard van Koten
• Journal of publication: Inorganic Chemistry
• Year of publication: 1998
• Journal volume: 37
• Pages of publication: 56 - 63
• a: 18.015 ± 0.006 Å
• b: 9.257 ± 0.006 Å
• c: 20.012 ± 0.005 Å
• α: 90°
• β: 109.63 ± 0.03°
• γ: 90°
• Cell volume: 3143 ± 2 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.084
• Residual factor for significantly intense reflections: 0.068
• Weighted residual factors for all reflections: 0.1783
• Weighted residual factors for significantly intense reflections: 0.1688
• Goodness-of-fit parameter for all reflections: 1.013
• Goodness-of-fit parameter for significantly intense reflections: 1.094
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No