Information card for entry 4322619

Structure parameters

• Formula: C14 H32 Cl Cu N7 Ni O7 S
• Calculated formula: C14 H30 Cl Cu N7 Ni O7 S
• Title of publication: Synthesis and Magnetic Properties of Four New (Cu-Ni)2 Tetranuclear Complexes of General Formula [Cu(oxpn)Ni(μ-NCS)(H2O)(aa)]2(X)2 (oxpn =N,N'-Bis(3-aminopropyl)oxamide; aa = Bidentate Amine; X = ClO4- or PF6-). Ferro- and Antiferromagnetic Alternation
• Authors of publication: Joan Ribas; Carmen Diaz; Ramon Costa; Javier Tercero; Xavier Solans; Mercé Font-Bardía; Helen Stoeckli-Evans
• Journal of publication: Inorganic Chemistry
• Year of publication: 1998
• Journal volume: 37
• Pages of publication: 233 - 239
• a: 8.407 ± 0.007 Å
• b: 12.779 ± 0.004 Å
• c: 14.081 ± 0.003 Å
• α: 63.25 ± 0.02°
• β: 88.62 ± 0.03°
• γ: 79.06 ± 0.04°
• Cell volume: 1323.1 ± 1.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1369
• Residual factor for significantly intense reflections: 0.0687
• Weighted residual factors for all reflections: 0.2603
• Weighted residual factors for significantly intense reflections: 0.182
• Goodness-of-fit parameter for all reflections: 1.049
• Goodness-of-fit parameter for significantly intense reflections: 1.094
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No