Information card for entry 4322678

Structure parameters

• Formula: C18 H48 F12 Fe N18 Ni3 P2
• Calculated formula: C54 H144 F36 Fe3 N54 Ni9 P6
• Title of publication: Bimetallic Assemblies [Ni(L)2]3[Fe(CN)6]X2 (L = Ethylenediamine, Trimethylenediamine; X = PF6-, ClO4-) with a Three-Dimensional Network Extended through FeII-CN-NiII Linkages
• Authors of publication: Nobuo Fukita; Masaaki Ohba; Hisashi Ōkawa; Kenji Matsuda; Hiizu Iwamura
• Journal of publication: Inorganic Chemistry
• Year of publication: 1998
• Journal volume: 37
• Pages of publication: 842 - 848
• a: 13.743 ± 0.001 Å
• b: 13.7428 Å
• c: 17.802 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 2911.8 ± 0.4 ų
• Cell temperature: 20 K
• Ambient diffraction temperature: 20 K
• Number of distinct elements: 7
• Space group number: 148
• Hermann-Mauguin space group symbol: R -3 :H
• Hall space group symbol: -R 3
• Residual factor for significantly intense reflections: 0.035
• Weighted residual factors for significantly intense reflections: 0.034
• Goodness-of-fit parameter for significantly intense reflections: 6.3
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKalpha
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No