Crystallography Open Database

Information card for entry 4322893

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Coordinates	4322893.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C53 H43 Cl2 N2 O4 P2 Re
Calculated formula	C53 H43 Cl2 N2 O4 P2 Re
Title of publication	Reaction of Organolithium Reagents with Tetracarbonyl[2-(phenyl-κC2'),pyridine-κN]rhenium(I): Isolation and Structural Characterization of Acyl Rhenate Species
Authors of publication	Jean-Pierre Djukic; Karl Heinz Dötz; Michel Pfeffer; André De Cian; Jean Fischer
Journal of publication	Inorganic Chemistry
Year of publication	1998
Journal volume	37
Pages of publication	3649 - 3651
a	20.747 ± 0.001 Å
b	14.515 ± 0.0009 Å
c	18.162 ± 0.002 Å
α	90°
β	121.196 ± 0.006°
γ	90°
Cell volume	4678.5 ± 0.7 Å³
Cell temperature	173 K
Ambient diffraction temperature	173 K
Number of distinct elements	7
Space group number	9
Hermann-Mauguin space group symbol	C 1 c 1
Hall space group symbol	C -2yc
Residual factor for all reflections	0.033
Residual factor for significantly intense reflections	0.029
Weighted residual factors for all reflections	0.061
Weighted residual factors for significantly intense reflections	0.041
Goodness-of-fit parameter for all reflections	1.564
Goodness-of-fit parameter for significantly intense reflections	1.061
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	Mo-Kα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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