Information card for entry 4322899

Structure parameters

• Formula: C10 H26 K O P Si2
• Calculated formula: C10 H26 K O P Si2
• SMILES: [K][O]1CCCC1.[P-]([Si](C)(C)C)[Si](C)(C)C
• Title of publication: A Convenient Synthetic Strategy toward Heavy Alkali Metal Bis(trimethylsilyl)phosphides: Crystal Structures of the Ladder-Type Polymers [A(thf)P(SiMe3)2]∞ (A = K, Rb, Cs)
• Authors of publication: Ulrich Englich; Karl Hassler; Karin Ruhlandt-Senge; Frank Uhlig
• Journal of publication: Inorganic Chemistry
• Year of publication: 1998
• Journal volume: 37
• Pages of publication: 3532 - 3537
• a: 6.4261 ± 0.0002 Å
• b: 12.4119 ± 0.0002 Å
• c: 21.5447 ± 0.0004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1718.41 ± 0.07 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0351
• Residual factor for significantly intense reflections: 0.0302
• Weighted residual factors for all reflections: 0.0676
• Weighted residual factors for significantly intense reflections: 0.066
• Goodness-of-fit parameter for all reflections: 1.012
• Goodness-of-fit parameter for significantly intense reflections: 1.04
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No