Information card for entry 4322921

Structure parameters

• Chemical name: bis((mu|3$-benziimidazole-2-thiolato-S,S,N)-(dicarbonyl-rhodium(i))- (chloride-dicarbonyl-rhodium(i))) dichloromethane solvate
• Formula: C23 H12 Cl4 N4 O8 Rh4 S2
• Calculated formula: C23 H12 Cl4 N4 O8 Rh4 S2
• Title of publication: Hydrogen Bonding and Isomerism Arising from the Coordination Modes of Bridging Benzimidazole-2-thiolate Ligands in Tetranuclear Rhodium Complexes
• Authors of publication: Cristina Tejel; B. Eva Villarroya; Miguel A. Ciriano; Andrew J. Edwards; Fernando J. Lahoz; Luis A. Oro; Maurizio Lanfranchi; Antonio Tiripicchio; Marisa Tiripicchio-Camellini
• Journal of publication: Inorganic Chemistry
• Year of publication: 1998
• Journal volume: 37
• Pages of publication: 3954 - 3963
• a: 21.389 ± 0.003 Å
• b: 21.389 ± 0.003 Å
• c: 29.359 ± 0.006 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 13431 ± 4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 88
• Hermann-Mauguin space group symbol: I 41/a :2
• Hall space group symbol: -I 4ad
• Residual factor for all reflections: 0.0537
• Residual factor for significantly intense reflections: 0.0463
• Weighted residual factors for all reflections: 0.1253
• Weighted residual factors for significantly intense reflections: 0.1179
• Goodness-of-fit parameter for all reflections: 1.062
• Goodness-of-fit parameter for significantly intense reflections: 1.073
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No