Information card for entry 4322992

Structure parameters

• Formula: C24 H64 Cl26 Nb6 O2 S8
• Calculated formula: C24 H56 Cl26 Nb6 O2 S8
• Title of publication: Synthesis, Structure, Hydrolysis, and Film Deposition Studies of Complexes of the Formula [NbCl4(S2R2)2][NbCl6]
• Authors of publication: Peggy J. McKarns; Mary Jane Heeg; Charles H. Winter
• Journal of publication: Inorganic Chemistry
• Year of publication: 1998
• Journal volume: 37
• Pages of publication: 4743 - 4747
• a: 27.658 ± 0.002 Å
• b: 14.309 ± 0.001 Å
• c: 19.843 ± 0.001 Å
• α: 90°
• β: 110.883 ± 0.001°
• γ: 90°
• Cell volume: 7337.2 ± 0.8 ų
• Cell temperature: 295 ± 2 K
• Ambient diffraction temperature: 295 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1092
• Residual factor for significantly intense reflections: 0.0404
• Weighted residual factors for all reflections: 0.0784
• Weighted residual factors for significantly intense reflections: 0.0654
• Goodness-of-fit parameter for all reflections: 0.882
• Goodness-of-fit parameter for significantly intense reflections: 1.023
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No