Information card for entry 4323048

Structure parameters

• Formula: C32 H54 N4 O6 W
• Calculated formula: C26.6667 H36 N2.66667 O6.66667 W1.33333
• Title of publication: Binucleating Coordination of N,N'-Ethylenebis(salicylideneamine) (H2salen) to Low-Valent Group 6 Carbonyl Complexes
• Authors of publication: Donald J. Darensbourg; Jennifer D. Draper
• Journal of publication: Inorganic Chemistry
• Year of publication: 1998
• Journal volume: 37
• Pages of publication: 5383 - 5386
• a: 8.432 ± 0.002 Å
• b: 14.7687 ± 0.0015 Å
• c: 18.4477 ± 0.0015 Å
• α: 106.907 ± 0.007°
• β: 90.904 ± 0.01°
• γ: 93.654 ± 0.012°
• Cell volume: 2192.1 ± 0.6 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1095
• Residual factor for significantly intense reflections: 0.0688
• Weighted residual factors for all reflections: 0.1889
• Weighted residual factors for significantly intense reflections: 0.1573
• Goodness-of-fit parameter for all reflections: 1.094
• Goodness-of-fit parameter for significantly intense reflections: 1.157
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No