Information card for entry 4323059

Structure parameters

• Formula: C54 H55 Cl7 P3 Rh Si4
• Calculated formula: C51.478 H55 Cl5.644 P3 Rh Si4
• Title of publication: Synthesis and Reactivity of Rhodium(I) and Iridium(I) Chloride Complexes of a Trisphosphinine
• Authors of publication: Nicolas Mézailles; Narcis Avarvari; Louis Ricard; François Mathey; Pascal Le Floch
• Journal of publication: Inorganic Chemistry
• Year of publication: 1998
• Journal volume: 37
• Pages of publication: 5313 - 5316
• a: 12.038 ± 0.001 Å
• b: 13.098 ± 0.001 Å
• c: 18.079 ± 0.002 Å
• α: 93.04 ± 0.02°
• β: 99.09 ± 0.02°
• γ: 101.66 ± 0.02°
• Cell volume: 2746 ± 0.5 ų
• Cell temperature: 123 K
• Ambient diffraction temperature: 123 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.055
• Residual factor for significantly intense reflections: 0.05
• Weighted residual factors for all reflections: 0.102
• Weighted residual factors for all reflections included in the refinement: 0.091
• Goodness-of-fit parameter for all reflections: 2.359
• Goodness-of-fit parameter for all reflections included in the refinement: 2.09
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: Mo-Kα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No