Information card for entry 4323166

Structure parameters

• Formula: C53 H81 Co Li N4 O4
• Calculated formula: C62 H44 Co Li N4 O5
• Title of publication: The Intra- and Intermolecular Oxidative Coupling of Ni(II)-meso-Octaethyl Mono(pyridine)-Tris(pyrrole) Complex Leading to CC Bonds: Pathways to Oligomeric Porphyrinogens
• Authors of publication: Raffaella Crescenzi; Euro Solari; Carlo Floriani; Angiola Chiesi-Villa; Corrado Rizzoli
• Journal of publication: Inorganic Chemistry
• Year of publication: 1998
• Journal volume: 37
• Pages of publication: 6044 - 6051
• a: 16.32 ± 0.005 Å
• b: 20.671 ± 0.006 Å
• c: 15.276 ± 0.004 Å
• α: 90 ± 0°
• β: 90 ± 0°
• γ: 90 ± 0°
• Cell volume: 5153 ± 3 ų
• Cell temperature: 25 K
• Ambient diffraction temperature: 295 K
• Number of distinct elements: 6
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.2428
• Residual factor for significantly intense reflections: 0.0634
• Weighted residual factors for all reflections: 0.3154
• Weighted residual factors for significantly intense reflections: 0.1561
• Goodness-of-fit parameter for all reflections: 0.925
• Goodness-of-fit parameter for significantly intense reflections: 1.176
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKa
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No